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Beilstein J. Org. Chem. 2016, 12, 1196–1202, doi:10.3762/bjoc.12.115
Graphical Abstract
Figure 1: Chemical structure of the photosensitizing chromophores benzophenone (BZP) and 2-benzoylthiophene (...
Figure 2: Chemical structure of tiaprofenic acid (TPA) and suprofen (SP).
Figure 3: Chemical structures of dyads 1–3.
Scheme 1: Formation of products 4 and 5 upon photolysis of dyads 1 and 2.
Figure 4: Diagnostic NOE interactions in compounds 4 and 5.
Figure 5: Decrease of the absorbance at 290 nm upon irradiation in CH2Cl2 under N2 for 1 (red circles), 2 (bl...
Figure 6: Transient absorption spectra for dyad 1 in CH2Cl2 1 μs after laser pulse (λexc = 355 nm). Inset: No...
Scheme 2: Photoreaction pathways generating biradical and singlet oxygen species of a sensitizer (S), like SP...
Figure 7: Time-resolved experiments at 1270 nm upon excitation at 308 nm of aerated CH2Cl2 solutions of 1–3, ...